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2011-Sustainable Industrial Processing Summit
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Editors: | Florian K |
Publisher: | Flogen Star OUTREACH |
Publication Year: | 2012 |
Pages: | 828 pages |
ISBN: | 978-0-9879917-0-6 |
ISSN: | 2291-1227 (Metals and Materials Processing in a Clean Environment Series) |
Recovery of nuclear materials and rare-earths from spent nuclear fuel was examined by sulfide process consisted of sulfurization and acid leaching steps using the simulated fuel oxides. After the oxidation of UO2 pellet to U3O8 powder by voloxidation treatment, rare-earth in the sample were reacted with CS2 at c.a. 673 K forming oxy-sulfides or sulfides, while uranium oxides remained without sulfurization. Then oxysulfides and sulfides were separated by dissolution into nitric acid and nuclear materials such as uranium and plutonium were recovered as oxides. The conditions for selective sulfurization were also discussed.